50ml-250ml Stirred Pressure Reactors

Description - Mini Stirred Autoclaves

The minimate series of miniature pressure reactors and autoclaves range from 50ml to 250ml. They are the preferred choice across the R&Ds & universities when researchers want to do high value small scale synthesis or when hazard levels are high. Such mini autoclaves and reactors are particularly useful in academic research when the space available in the lab is small, or when portability of the system is important. This standard mini reactor series comes in SS table top mounting with heating, cooling & stirring arrangement, maintenance free zero leakage coupling, quick opening clamp design, inlet-outlet valves, pressure gauge, safety rupture disc & SS control panel with programmable temperature & speed controller. Country specific U stamp, PED, CRN, DOSH, Australian worksafe certified units can be supplied with many other optional accessories listed below for improved safety, features & versatility. SS316 reactors rated for 100 bar @ 300°C are standard models with quickest production lead times and can optionally be manufactured for upto 350bar & 500°C in other material of construction.

50ml High Pressure Autoclave Standard Models

ModelA 1213A 1215A 1223A 1225A 1233A 1235
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)404040404040
Vessel Internal Height (mm)636363636363
Min. Stirrable Volume (ml)202020202020
Enquiry

100ml High Pressure Autoclave Standard Models

ModelA 1313A 1315A 1323A 1325A 1333A 1335
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)404040404040
Vessel Internal Height (mm)838383838383
Min. Stirrable Volume (ml)202020202020
Enquiry

250ml High Pressure Autoclave Standard Models

ModelA 1413A 1415A 1423A 1425A 1433A 1435
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C 500°C300°C 500°C300°C 500°C
Vessel I/D (mm)656565656565
Vessel Internal Height (mm)808080808080
Min. Stirrable Volume (ml)505050505050
Enquiry

Technical specification for High Pressure Autoclave Standard Models

Description Standard Optional
Material of Construction SS 316 wetted parts SS 316L, Hastelloy C 276, Hastelloy C 22, Hastelloy B, Monel 400, Inconel 600, Inconel 625, Nickel 200, Titanium Gr. 2, Zirconium 702, Tantalum
Head Mounting Style Removable head and vessel design Fixed head with manual vessel raising lowering
Heating Type Electrical ceramic band heater with cladding & insulation & heater temperature control for 500°C Electrical cast heater ex-proof, IIB + H2 certified
Welded SS 304 jacket with insulation
Welded SS 304 jacket with electrical ceramic heater
Motor ⅛ hp AC motor with 100-1450 RPM ¼ hp ex-proof gas group IIB (Zone 1)
¼ hp ex-proof gas group IIC (Zone 1)
¼ hp ex-proof CE ATEX certified II 2G Ex de IIC T4
¼ hp ex-proof CSA certified Class 1 Div 2
⅛ hp compact in-line brushless DC motor
RPM upto 3000
Shaft Sealing Zero leakage magnetic drive coupling M8 with 0.8 Nm torque Zero leakage magnetic drive coupling M20 with 2 Nm torque
Stirrer 4 bladed turbine stirrer Hollow shaft with gas induction Impeller
Ruston turbine
Paddle
Propeller
Standard Nozzles, Valves & Fittings External Valves & Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, solenoid valve at inlet of cooling coil, vent needle valve (All needle valves ⅛" size)
Internal Fittings:
Serpentine cooling coil, dip tube, thermowell with RTD PT100 temperature sensor
Gasket PTFE up to 300°C Metallic grafoil gasket up to 500°C
Closure Type Split clamp with clamp bolts Threaded cap with FKM (Viton)'O' ring up to 225°C
Threaded cap with FFKM (Kalrez) 'O' ring up to 275°C
Control Panel SS control panel with programmable PID temperature controller with high temperature alarm and variable frequency drive for motor speed control Ex-proof gas group IIA/IIB zone 1 certified
Ex-proof gas group IIC zone 1 certified
Touch screen
Power Supply 1Ø, 220 V AC, 50 / 60 Hz Different power supply options may be possible on request
Mounting Table Top Floor stand
Certifications By Amar Design approval as per ASME code by notified body
CE-PED 2014/68/EU
ASME U stamp coded
ATEX certified reactor 2014/34/EU
CE marked panel & electrical parts
UL/CSA marked panel & electrical parts

Optional Accessories

Note: All accessories may not be applicable for above models.

Optional Accessories

Note: All accessories may not be applicable for above models.