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2l Hastelloy
Autoclave

100 bar design pressure at 300°C temperature
Interchangeable solid shaft turbine stirrer and hollow shaft gas induction impeller
100ml detachable Sampling pot with cooling provision mounted on sampling valve
Ø50mm & 2 feet Long Hast C distillation column
0.2 m2 Hastelloy C Condenser for distillation / condensation
1L Hastelloy C Receiver pot at the outlet of condenser
1L Hastelloy C High Pressure Liquid / Catalyst Slurry /Gas charging system

High Pressure
Vessel

250 ml, 300 bar, 200°C vessel
Two sapphire windows
Ultrasonic probe (20KHz & 120W) fitted in the vessel, provision for ultrasound horn (½ inch) insertion
Profiling software for real time logging and analysis
VFD Controlled high pressure CO2 Pump with flow rate upto 2 lph
SS316 product collection vessel connected to the bottom of High pressure vessel

Pilot Plant
Reactor Vessel

10 liters X 4 net filling capacity
FV to 5 bar pressure at -10°C to +150°C
Light and sight glass round on body for observing, capturing photos and video recording of the reaction
Common control panel with individual pressure & temperature indicators and variable frequency drives

High Pressure Vessel for Formation
& Dissociation Gas Hydrates

Volume-750cc
Design Pressure-4000 Psi
Design temperature-(-100°C to 500°C)
Temperature Accuracy-±0.10°C
Removable Lid (with round Quartz window for viewing contents)
Microwave Source with Wave Guide, Microwave circulator, Microwave Dual direction decoupler, Rectangular – Circular Transducer, Microwave three stub turner
Software for monitoring the pressure-temperature variation, Hydrate stability Zone and the rate of dissociation of gas hydrates

100 ltr
Pilot Plant

Hydrogenation
Pilot Plant

Design pressure 50 bar @250°C
Ex-proof gas group IIC zone 1 certified Control panel with programmable P.I.D temperature controller
Catalyst filtration unit with flow rate 300ltr/hr
5L high-pressure charging pot for injecting liquids/gas/catalyst during the reaction under pressure
Torque wrench for uniform tightening, easy operation & ensuring leak tightness.

Multiple Catalyst
Screening System

6 Nos. Multiple Catalyst Screening 100ml Parallel Autoclaves
Material of construction: SS316, Hastelloy C22 & Inconel
Digital gas Mass Flow Controller mounted inside Explosion proof IIC enclosure
100ml agitated High Pressure Liquid / Catalyst Slurry charging pot for injecting liquids / Catalyst slurry during the reaction under pressure
Common Digital temperature indicator & RPM indicator for all reactors in flameproof enclosure
Common SCADA Software for online display trends, Data logging

Reactor for
Hydrogen Production

100 ltr Pilot Plant

Helical Static Mixer Enclosed in
Double Pipe Heat Exchanger

Wetted Parts: Hastelloy C276
Design Pressure: 50 bar
Temperature Range: -40 to +250°C
High surface to volume ratio
Effective mixing with minimum pressure drop
Tube-In-Tube Type Design
Capability of dosing aggressive chemicals at high pressure with pulseless dosing
Application: Nitration, Diazotization, Liquid-Liquid Extraction, synthesis of high performance chemicals
Multiple sampling ports provided along the length for kinetic study

Autoclaves for
Reaction Calorimetry

Lab Agitated Nutsche
Filter & Dryer - ANFD