10ltr-100ltr Stirred Pressure Reactors

Description - Pilot Reactors

Pilotmate series of high pressure stirred autoclaves include 10ltrs to 100ltrs reactor volumes. This range is very common for piloting purpose before scale up once the process is developed on a minimate or labmate. This scale is often used for production purpose of high value small quantity requirement. This series as standard comes with SS trolley mounting with heating, cooling, & stirring arrangements, zero leakage high torque magnetic coupling, quick opening clamp design, inlet, outlet & charging valves, bottom drain valve, pressure gauge, safety rupture disc & SS control panel with programmable temperature & speed controller. Country specific U stamp, PED, CRN, DOSH certified units can be supplied with many other optional accessories listed below for improved safety, features & versatility. Customized automated & exproof pilot plants are developed using these volumes with turnkey solutions. SS316 material with 100 bar @ 300°C rating are quickest available running models with options upto 350bar & 500°C & other materials.

10 ltr High Pressure AutoVclave Standard Models

ModelA 3113A 3115A 3123A 3125A 3133A 3135
Design Pressure100 bar100 bar200 bar200 bar350 bar350 bar
Design Temperature300°C500°C300°C500°C300°C500°C
Vessel I/D (mm)183183183183183183
Vessel Internal Height (mm)420420420420420420
Min. Stirrable Volume (ltr)111111
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20 ltr High Pressure AutoVclave Standard Models

ModelA 3213A 3215A 3223A 3225
Design Pressure100 bar100 bar200 bar200 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)248248248248
Vessel Internal Height (mm)495495495495
Min. Stirrable Volume (ltr)2.62.62.62.6
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25 ltr High Pressure AutoVclave Standard Models

ModelA 3313A 3315A 3323A 3325
Design Pressure100 bar100 bar200 bar200 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)248248248248
Vessel Internal Height (mm)595595595595
Min. Stirrable Volume (ltr)2.62.62.62.6
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50 ltr High Pressure AutoVclave Standard Models

ModelA 3403A 3405A 3413A 3415
Design Pressure50 bar50 bar100 bar100 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)355355343343
Vessel Internal Height (mm)558558600600
Min. Stirrable Volume (ltr)6666
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100 ltr High Pressure AutoVclave Standard Models

ModelA 3503A 3505A 3513A 3515
Design Pressure50 bar50 bar100 bar100 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)456456440440
Vessel Internal Height (mm)699699735735
Min. Stirrable Volume (ltr)12121212
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Technical specification for High Pressure AutoVclave Standard Models

DescriptionStandardOptional
Material of ConstructionSS 316 wetted partsSS 316L, Hastelloy C 276, Hastelloy C 22, Hastelloy B, Monel 400, Inconel 600, Inconel 625, Nickel 200, Titanium Gr. 2, Zirconium 702, Tantalum lined
Head Mounting StyleRemovable head and vessel designFixed head with pneumatic vessel raising lowering (10ltr to 25ltr)
Fixed head with hydraulic vessel raising lowering (50ltr & 100ltr)
Fixed head with pneumatic vessel raising lowering & tilting (10ltr to 25ltr)
Fixed head with hydraulic vessel raising lowering & tilting (50ltr & 100ltr)
Heating TypeElectrical ceramic band heater with cladding & insulation & heater temperature control for 500°CElectrical cast ex-proof, IIB + H2 certified
Welded SS 304 jacket with insulation
Welded SS 304 jacket with electrical ceramic heater
Limpet coil SS 304 with insulation (20ltr to 100ltr)
Motor ¼ hp AC motor for 10ltr, 20ltr & 25ltr locked to 750 rpm
½ hp AC motor for 50ltr & 100ltr locked to 500 rpm
1 hp / 2hp / 3hp Ex-proof gas group IIB (Zone 1) XB
1 hp / 2hp / 3hp Ex-proof gas group IIC (Zone 1) XC
1 hp / 2hp / 3hp Ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ
1 hp / 2hp / 3hp Ex-proof CSA certified Class 1 Div 2
¼ hp compact in-line brushless DC motor
Gearbox upto 440 rpm
Shaft SealingZero leakage magnetic drive coupling:
M20 with 2 Nm torque
Zero leakage magnetic drive coupling:
M120 with 12 Nm torque (for 10 to 25 ltr)
M200 with 20 Nm torque (upto 750 rpm, for 10 to 25 ltr)
M400 with 40 Nm torque (upto 750 rpm)
Stirrer2 stage 6 bladed turbine stirrerHollow shaft with gas induction Impeller
Anchor (Serpentine cooling coil, max 100 rpm)
Spiral (No cooling coil, max 100 rpm)
Ruston turbine
Paddle
Propeller
Standard Nozzles, Valves & FittingsExternal Valves & Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, vent needle valve, ball valve for powder/liquid inlet with funnel, flush bottom valve
Internal Fittings:
Helical cooling coil, dip tube, thermowell with RTD PT100 temperature sensor
Serpentine cooling coil
GasketPTFE up to 300°CMetallic grafoil gasket up to 500°C
Closure TypeSplit clamp with clamp bolts
Control PanelSS control panel with programmable PID temperature controller with high temperature alarm and variable frequency drive for motor speed controlEx-proof gas group IIA/IIB zone 1 certified
Ex-proof gas group IIC zone 1 certified
Touch screen
Power Supply1Ø, 220 V AC, 20 amp, 50 / 60 Hz for 10 ltr
3Ø, 440 V AC, 25 amp, 50 / 60 Hz for 20 ltr to 100 ltr
Different power supply options may be possible on request
MountingSS TrolleyFloor Stand
CertificationsBy AmarDesign approval as per ASME code by notified body
CE-PED 2014/68/EU
ASME U stamp coded
ATEX certified reactor 2014/34/EU
CE marked panel & electrical parts
UL/CSA marked panel & electrical parts

Optional Accessories

Note: All accessories may not be applicable for above models.

Optional Accessories

Note: All accessories may not be applicable for above models.